cis-3--1-phenyltetralin hydrochloride

Base Information

Chemical Name:cis-3--1-phenyltetralin hydrochloride
CAS No.:74716-79-3
Molecular Formula:C₂₁H₂₅N*ClH
Molecular Weight:327.897
Hs Code.:

cis-3-<N-methyl-N-(cyclopropylmethyl)amino>-1-phenyltetralin hydrochloride

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-3--1-phenyltetralin hydrochloride

Chemical Property:

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Technology Process of cis-3--1-phenyltetralin hydrochloride

There total 22 articles about cis-3--1-phenyltetralin hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 80232-36-6
3--3,4-dihydro-1-phenylnaphthalene hydrochloride

: 74716-79-3,80232-35-5,80232-37-7
trans-3--1-phenyltetralin hydrochloride

: 74716-79-3,80232-35-5,80232-37-7
cis-3--1-phenyltetralin hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00345a005

Reference yield: 60.0%

: 80232-36-6
3--3,4-dihydro-1-phenylnaphthalene hydrochloride

: 74716-79-3,80232-35-5,80232-37-7
trans-3--1-phenyltetralin hydrochloride

: 74716-79-3,80232-35-5,80232-37-7
cis-3--1-phenyltetralin hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00345a005

Reference yield:

: 718-08-1
ethyl 3-oxo-4-phenylbutyrate

: 74716-79-3,80232-35-5,80232-37-7
trans-3--1-phenyltetralin hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: methanol / 25 °C

2: NaBH₃CN, HCl gas / methanol

3: pyridine / benzene / 2 h / 25 °C

4: 0.2 N NaOH / tetrahydrofuran / 1 h / 25 °C

5: 41 percent / anhydrous HF / 10 h

6: diethyl ether / 6 h / 25 °C

7: H₂, 60percent HClO₄ / 10percent Pd/C / ethanol / 2585.7 Torr

8: 1.) H₂, 60percent HClO₄, 2.) LiAlH₄ / 1.) 10percent Pd/C / 1.) EtOH, 50 psi, 2.) THF

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; perchloric acid; hydrogen fluoride; hydrogen; sodium cyanoborohydride; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; benzene;
DOI:10.1021/jm00345a005