3',4'-dideoxykanamycin A

Base Information

Chemical Name:3',4'-dideoxykanamycin A
CAS No.:57539-39-6
Molecular Formula:C₁₈H₃₆N₄O₉
Molecular Weight:452.505
Hs Code.:

Synonyms:

Suppliers and Price of 3',4'-dideoxykanamycin A

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3',4'-dideoxykanamycin A

Chemical Property:

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Technology Process of 3',4'-dideoxykanamycin A

There total 11 articles about 3',4'-dideoxykanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 80860-40-8
3',4'-dideoxy-3'-enekanamycin A

: 57539-39-6,75829-17-3
3',4'-dideoxykanamycin A

Guidance literature:: With hydrogen; platinum(IV) oxide; In water; for 2h; under 760 Torr;
DOI:10.1248/cpb.29.3464

Reference yield:

: 80860-37-3
2',3',2''-tri-O-benzoyl-4'',6''-O-cyclohexylidene-4'-methylsulfonyl-tetra-N-tert-butoxycarbonylkanamycin A

: 57539-39-6,75829-17-3
3',4'-dideoxykanamycin A

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / sodium methoxide / methanol; CHCl₃ / 0 °C

2: 1.56 g / pyridine / 2 h / Ambient temperature

3: 61 percent / sodium iodide, sodium acetate, acetic acid / acetone / 4 h / Heating

4: 1.) α-toluenesulfonyl chloride / 1.) pyridine, 5 deg C, 1 h, 2.) pyridine, 90 deg C, 1 h

5: 78 percent / sodium methoxide / methanol / 0.5 h / Ambient temperature

6: 75 percent / 95percent trifluoroacetic acid / 0.17 h / Ambient temperature

7: 90 percent / hydrogen / platinium oxide / H₂O / 2 h / 760 Torr

With pyridine; hydrogen; sodium methylate; sodium acetate; acetic acid; trifluoroacetic acid; sodium iodide; benzenesulfonyl chloride; platinum(IV) oxide; In methanol; chloroform; water; acetone;
DOI:10.1248/cpb.29.3464

Reference yield:

: 80860-36-2
2',3',2''-tri-O-benzoyl-4'',6''-O-cyclohexylidene-tetra-N-tert-butoxycarbonylkanamycin A

: 57539-39-6,75829-17-3
3',4'-dideoxykanamycin A

Guidance literature:: Multi-step reaction with 8 steps

1: 89 percent / pyridine / 3 h / Ambient temperature

2: 88 percent / sodium methoxide / methanol; CHCl₃ / 0 °C

3: 1.56 g / pyridine / 2 h / Ambient temperature

4: 61 percent / sodium iodide, sodium acetate, acetic acid / acetone / 4 h / Heating

5: 1.) α-toluenesulfonyl chloride / 1.) pyridine, 5 deg C, 1 h, 2.) pyridine, 90 deg C, 1 h

6: 78 percent / sodium methoxide / methanol / 0.5 h / Ambient temperature

7: 75 percent / 95percent trifluoroacetic acid / 0.17 h / Ambient temperature

8: 90 percent / hydrogen / platinium oxide / H₂O / 2 h / 760 Torr

With pyridine; hydrogen; sodium methylate; sodium acetate; acetic acid; trifluoroacetic acid; sodium iodide; benzenesulfonyl chloride; platinum(IV) oxide; In methanol; chloroform; water; acetone;
DOI:10.1248/cpb.29.3464