(Lu(2,4,6-triisopropylbenzoate)3)n

Base Information

Chemical Name:(Lu(2,4,6-triisopropylbenzoate)3)n
CAS No.:884337-62-6
Molecular Formula:C₄₈H₆₉LuO₆
Molecular Weight:917.039
Hs Code.:

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Chemical Property of (Lu(2,4,6-triisopropylbenzoate)3)n

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Technology Process of (Lu(2,4,6-triisopropylbenzoate)3)n

There total 1 articles about (Lu(2,4,6-triisopropylbenzoate)3)n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: Lu(N(SiMe₃)2)3

: 49623-71-4
2,4,6-triisopropylbenzoic acid

: 884337-62-6
(Lu(2,4,6-triisopropylbenzoate)3)n

Guidance literature:: In tetrahydrofuran; byproducts: HN(SiMe3)2; under vac.; to a soln. of Lu-contg. compd. (1.00 mmol) in THF was slowlyadded a soln. of carboxylic acid (3.00 mmol) in THF at -45°C; st irring at ambient temp. overnight (16 h); the solvent and volatiles were removed in vac.; solid was washed severaltimes with hexane; drying for several hours; elem. anal.;
DOI:10.1021/om060052i

Reference yield: 37.0%

: 884337-62-6
(Lu(2,4,6-triisopropylbenzoate)3)n

: 75-24-1
trimethylaluminum

: Lu[(2,4,6-triisopropylbenzoate)2(μ-AlMe2)]2[(μ-Me)2AlMe2]

Guidance literature:: In hexane; in a glovebox, AlMe3 (3.00 mmol) was added to carboxylate complex (0.50 mmol) suspended in hexane; stirring overnight at ambient temp.; the mixt. was centrifuged; the insol. compd. was washed several times with hexane; drying for several hours; elem. anal.; other compds. were also obtained;
DOI:10.1021/om060052i