C₃₅H₅₁NO₆Si

Base Information

• Chemical Name: C₃₅H₅₁NO₆Si
• CAS No.: 1293966-38-7
• Molecular Formula: C₃₅H₅₁NO₆Si
• Molecular Weight: 609.879
• Mol file: 1293966-38-7.mol

Synonyms:

Chemical Property of C₃₅H₅₁NO₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₅₁NO₆Si

There total 13 articles about C₃₅H₅₁NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H22O3 (1255763-92-8) → C35H51NO6Si (1293966-38-7)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

2: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

3: Inert atmosphere

With dihydrogen peroxide; In methanol; dichloromethane; water; 1: Aldol condensation;

DOI:10.1021/ol2007296

Reference yield:

C16H34O2S2Si (1293966-60-5) → C35H51NO6Si (1293966-38-7)

Guidance literature:

Multi-step reaction with 8 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 4 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 °C / Inert atmosphere

5.1: water; calcium carbonate; methyl iodide / acetonitrile / 24 h / 40 °C / Inert atmosphere

6.1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

7.1: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

8.1: Inert atmosphere

With tetrabutyl ammonium fluoride; water; dihydrogen peroxide; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; calcium carbonate; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil; 4.2: Wittig reaction / 6.1: Aldol condensation;

DOI:10.1021/ol2007296

Reference yield:

C12H28O2Si (1293966-59-2) → C35H51NO6Si (1293966-38-7)

Guidance literature:

Multi-step reaction with 10 steps

1.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 4 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C / Inert atmosphere

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.2: 0 °C / Inert atmosphere

7.1: water; calcium carbonate; methyl iodide / acetonitrile / 24 h / 40 °C / Inert atmosphere

8.1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

9.1: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

10.1: Inert atmosphere

With n-butyllithium; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; calcium carbonate; methyl iodide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil; 6.2: Wittig reaction / 8.1: Aldol condensation;

DOI:10.1021/ol2007296

upstream raw materials:

C₁₆H₂₂O₃

C₁₂H₂₈O₂Si

C₁₂H₂₆O₂Si

C₁₆H₃₄O₂S₂Si

Downstream raw materials:

C₂₅H₄₂O₅Si

C₄₄H₆₆O₉SSi

C₃₇H₆₀O₉Si

C₄₃H₇₄O₉Si₂