Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide

Base Information

• Chemical Name: Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide
• CAS No.: 6152-23-4
• Molecular Formula: C10H13 N3 O2
• Molecular Weight: 207.232
• UNII: 6F8AT9667O
• Nikkaji Number: J777.092H
• Wikidata: Q27264813

Synonyms:NSC-96477;UNII-6F8AT9667O;(+)-5-(alpha-Phenylethyl)semioxamazide;6F8AT9667O;5-(alpha-Phenylethyl)semioxamazide, D-;5-(alpha-Phenylethyl)semioxamazide, (+)-;6152-23-4;Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide;5-(alpha-Phenylethyl)semioxamazide D-form [MI];Semioxamazide, 5-(alpha-methylbenzyl)-, (+)-;N-Amino-N'-[(R)-alpha-methylbenzyl]oxamide;(+)-5-(.ALPHA.-PHENYLETHYL)SEMIOXAMAZIDE;5-(.ALPHA.-PHENYLETHYL)SEMIOXAMAZIDE, D-;5-(.ALPHA.-PHENYLETHYL)SEMIOXAMAZIDE, (+)-;Q27264813;5-(.ALPHA.-PHENYLETHYL)SEMIOXAMAZIDE D-FORM [MI];SEMIOXAMAZIDE, 5-(.ALPHA.-METHYLBENZYL)-, (+)-

Chemical Property of Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide

Chemical Property:

• XLogP3: 1
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 207.100776666
• Heavy Atom Count: 15
• Complexity: 237

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C1=CC=CC=C1)NC(=O)C(=O)NN
• Isomeric SMILES: C[C@H](C1=CC=CC=C1)NC(=O)C(=O)NN

Technology Process of Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide

There total 1 articles about Acetic acid, 2-oxo-2-(((1R)-1-phenylethyl)amino)-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-1-phenyl-ethyl-amine (3886-69-9) + oxalic acid diethyl ester (95-92-1) → (R)-2-hydrazinyl-2-oxo-N-(1-phenylethyl)acetamide (6152-23-4)

Guidance literature:

With hydrazine hydrate;

DOI:10.1021/jo01147a007

Reference yield: 92.0%

4-formyl[2.2]paracyclophane (36325-27-6,37044-38-5,729-30-6,147127-97-7) + (R)-2-hydrazinyl-2-oxo-N-(1-phenylethyl)acetamide (6152-23-4) → C27H27N3O2

Guidance literature:

With iodine; In benzene; at 20 ℃; for 168h;

DOI:10.1016/j.tetasy.2010.05.033

Reference yield: 66.0%

spiro[4.4]nonane-1,6-dione (21932-23-0,27723-43-9,36551-90-3) + (R)-2-hydrazinyl-2-oxo-N-(1-phenylethyl)acetamide (6152-23-4) → C29H34N6O4

Guidance literature:

With iodine; In dichloromethane; Inert atmosphere; Reflux;

upstream raw materials:

(R)-1-phenyl-ethyl-amine

oxalic acid diethyl ester

Downstream raw materials:

1R,4S-(-)-bicyclo<2.2.2>octane-2,5-dione

C₃₄H₄₀N₆O₈

C₃₄H₄₀N₆O₈

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