[(diphenyl(4-penten-1-yl)phosphine]CuCl

Base Information

• Chemical Name: [(diphenyl(4-penten-1-yl)phosphine]CuCl
• CAS No.: 352512-90-4
• Molecular Formula: C₁₇H₁₉ClCuP
• Molecular Weight: 353.311
• Mol file: 352512-90-4.mol

Synonyms:

Chemical Property of [(diphenyl(4-penten-1-yl)phosphine]CuCl

Chemical Property:

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Useful:

Technology Process of [(diphenyl(4-penten-1-yl)phosphine]CuCl

There total 1 articles about [(diphenyl(4-penten-1-yl)phosphine]CuCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-pentenyldiphenylphosphine (3053-61-0) + copper(l) chloride → [(diphenyl(4-penten-1-yl)phosphine]CuCl (352512-90-4)

Guidance literature:

In tetrahydrofuran; under N2; the phosphine was added to a suspn. of CuCl in THF, the mixt. was stirred for 6 h at 25°C; the mixt. was evapd. in vac., the residue was extd. with CHCl3 by flash column chromy. on SiO2, the solvent was evapd. in vac.;

DOI:10.1021/om000592u

upstream raw materials:

4-pentenyldiphenylphosphine