Technology Process of C37H40N4O11S
There total 7 articles about C37H40N4O11S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen bromide / dichloromethane
2.1: palladium 10% on activated carbon; hydrogen; acetic acid / 5 h / 95 °C / 1520.1 Torr
3.1: pyridine / dichloromethane / Inert atmosphere
3.2: 0.75 h / 20 °C / Inert atmosphere
4.1: triethylamine / dichloromethane / 20 °C
With
pyridine; palladium 10% on activated carbon; hydrogen bromide; hydrogen; acetic acid; triethylamine;
In
dichloromethane;
DOI:10.1016/j.ejmech.2011.06.004
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane
2: triethylamine / dichloromethane / 20 °C
With
triethylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.ejmech.2011.06.004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2: trifluoroacetic acid / dichloromethane
3: triethylamine / dichloromethane / 20 °C
With
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.ejmech.2011.06.004
