disulfanediyldi-acetic acid di-p-toluidide

Base Information

• Chemical Name: disulfanediyldi-acetic acid di-p-toluidide
• CAS No.: 7267-65-4
• Molecular Formula: C₁₈H₂₀N₂O₂S₂
• Molecular Weight: 360.501
• Mol file: 7267-65-4.mol

Synonyms:

Chemical Property of disulfanediyldi-acetic acid di-p-toluidide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of disulfanediyldi-acetic acid di-p-toluidide

There total 6 articles about disulfanediyldi-acetic acid di-p-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-mercapto-N-p-tolylacetamide (34282-30-9) → disulfanediyldi-acetic acid di-p-toluidide (7267-65-4)

Guidance literature:

With hydrogenchloride; ethanol; iron(III) chloride;

DOI:10.1111/1468-0289.00200

Reference yield:

4-(S-acetyl-thioacetamido)-toluene (884815-91-2) → disulfanediyldi-acetic acid di-p-toluidide (7267-65-4)

Guidance literature:

With water; potassium carbonate; In methanol; at 90 ℃; for 1h; Inert atmosphere;

DOI:10.1002/cmdc.202100618

Reference yield:

p-toluidine (106-49-0,12221-03-3) → disulfanediyldi-acetic acid di-p-toluidide (7267-65-4)

Guidance literature:

Multi-step reaction with 3 steps

1: water

2: 10 percent ammonia

3: iron chloride; HCl; alcohol

With hydrogenchloride; ammonium hydroxide; ethanol; water; iron(III) chloride;

DOI:10.1111/1468-0289.00200

upstream raw materials:

2-mercapto-N-p-tolylacetamide

carbamoylsulfanyl-acetic acid p-toluidide

p-toluidine

N-(p-tolyl)-2-chloroacetamide

Downstream raw materials:

N-(4-methylphenyl)-2-(4-methylphenylamino)-2-thioxoacetamide

Refernces