[Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh₃)2(CO)]

Base Information

• Chemical Name: [Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh₃)2(CO)]
• CAS No.: 1307316-11-5
• Molecular Formula: C₅₂H₄₂ClN₃OP₂RuS
• Molecular Weight: 955.461

Synonyms:

Chemical Property of [Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh₃)2(CO)]

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Technology Process of [Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh₃)2(CO)]

There total 1 articles about [Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh₃)2(CO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) (157072-60-1,61521-25-3,166941-05-5,16971-33-8) + p-chloroacetophenone phenylthiosemicarbazone → [Ru(para-chloroacetophenone thiosemixcarbazone(-2H))(PPh3)2(CO)] (1307316-11-5)

Guidance literature:

With LiBr; NaOAc; In methanol; LiBr, NaOAc, and ligand added to MeOH soln. of Ru compd. (1:2:2:1 molar ratio), refluxed for 5 h (N2 flow); filtered off, washed(MeOH), dried (vac.), elem. anal.;

DOI:10.1016/j.inoche.2011.02.006

upstream raw materials:

(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)

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