Technology Process of C56H81IO8Si2
There total 5 articles about C56H81IO8Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) SO3*pyridine, NEt3, 2) NaN(TMS)2 / 1) CH2Cl2, DMSO, 0 deg C, 2 h, 2) THF, 0 deg C, 1 h
2: 1) 9-BBN, 2) NaOH, H2O2 / 1) THF, 0 deg C, 2 h, 2) 0 deg C, 1 h
3: NEt3 / CH2Cl2 / 0.33 h / 0 °C
4: NaI / acetone / 12 h / 50 °C
With
sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; pyridine-SO3 complex; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; sodium iodide;
In
dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NEt3 / CH2Cl2 / 0.33 h / 0 °C
2: NaI / acetone / 12 h / 50 °C
With
triethylamine; sodium iodide;
In
dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) 9-BBN, 2) NaOH, H2O2 / 1) THF, 0 deg C, 2 h, 2) 0 deg C, 1 h
2: NEt3 / CH2Cl2 / 0.33 h / 0 °C
3: NaI / acetone / 12 h / 50 °C
With
sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; triethylamine; sodium iodide;
In
dichloromethane; acetone;