1,3-dimesitylbenzothiophene

Base Information

• Chemical Name: 1,3-dimesitylbenzothiophene
• CAS No.: 128709-95-5
• Molecular Formula: C₂₆H₂₆S
• Molecular Weight: 370.558

Synonyms:

Chemical Property of 1,3-dimesitylbenzothiophene

Chemical Property:

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Technology Process of 1,3-dimesitylbenzothiophene

There total 1 articles about 1,3-dimesitylbenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1,2-(2,4,6-trimethylbenzoyl)benzene (4497-23-8) → 1,3-dimesitylbenzothiophene (128709-95-5)

Guidance literature:

With tetraphosphorus decasulfide; sodium hydrogencarbonate; In xylene; for 5h; Heating;

DOI:10.1055/s-1990-26976

Reference yield: 3.7%

1,3-dimesitylbenzothiophene (128709-95-5) → 1,3-Dimesitylbenzothiophen-4,5-chinon (128709-96-6) + 1,3-Dimesitylbenzothiophen-4,7-chinon (128709-97-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 72h; Ambient temperature;

Reference yield: 2.4%

N-phenyl-maleimide (941-69-5) + 1,3-dimesitylbenzothiophene (128709-95-5) → (4R,7S,8S,9R)-4,7-Dihydro-1,3-dimesityl-N-phenyl-4,7-ethanobenzothiophen-8,9-dicarboximid (128710-00-9)

Guidance literature:

In toluene; for 48h; Heating;

upstream raw materials:

1,2-(2,4,6-trimethylbenzoyl)benzene

Downstream raw materials:

(4R,7S,8S,9R)-4,7-Dihydro-1,3-dimesityl-N-phenyl-4,7-ethanobenzothiophen-8,9-dicarboximid

1,3-Dimesitylbenzothiophen-4,5-chinon

1,3-Dimesitylbenzothiophen-4,7-chinon

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