HCl*Phe-Phe-Gly-Phe-Met-NH₂

Base Information

Chemical Name:HCl*Phe-Phe-Gly-Phe-Met-NH₂
CAS No.:82816-83-9
Molecular Formula:C₃₄H₄₂N₆O₅S*ClH
Molecular Weight:683.272
Hs Code.:

Synonyms:

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Chemical Property of HCl*Phe-Phe-Gly-Phe-Met-NH₂

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Technology Process of HCl*Phe-Phe-Gly-Phe-Met-NH₂

There total 9 articles about HCl*Phe-Phe-Gly-Phe-Met-NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 82816-79-3
Boc-Phe-Phe-Gly-Phe-Met-NH₂

: 82816-83-9
HCl*Phe-Phe-Gly-Phe-Met-NH₂

Guidance literature:: With hydrogenchloride; acetic acid; for 0.5h;

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 82816-83-9
HCl*Phe-Phe-Gly-Phe-Met-NH₂

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / 1.) triethylamine (TEA), 2.) N-hydroxybenztriazole (HOBt), N,N'-dicyclohexylcarbodiimide (DCC) / dimethylformamide / 16 h

2: 76 percent / methanolic NH₃ / 48 h / Ambient temperature

3: 95 percent / 4 M HCl / ethyl acetate / 0.25 h / Ambient temperature

4: 78 percent / 1.) triethylamine (TEA), 2.) N-hydroxybenztriazole (HOBt), N,N'-dicyclohexylcarbodiimide (DCC) / dimethylformamide / 16 h / Ambient temperature

5: 79 percent / 4 M HCl, acetic acid / 0.5 h

With hydrogenchloride; ammonia; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 56063-15-1
Boc-Phe-Met-NH₂

: 82816-83-9
HCl*Phe-Phe-Gly-Phe-Met-NH₂

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 4 M HCl / ethyl acetate / 0.25 h / Ambient temperature

2: 78 percent / 1.) triethylamine (TEA), 2.) N-hydroxybenztriazole (HOBt), N,N'-dicyclohexylcarbodiimide (DCC) / dimethylformamide / 16 h / Ambient temperature

3: 79 percent / 4 M HCl, acetic acid / 0.5 h

With hydrogenchloride; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In ethyl acetate; N,N-dimethyl-formamide;