(trans-1,4-diphenylcyclohexane)tricarbonylchromium

Base Information

Chemical Name:(trans-1,4-diphenylcyclohexane)tricarbonylchromium
CAS No.:98859-22-4
Molecular Formula:C₂₁H₂₀CrO₃
Molecular Weight:372.384
Hs Code.:

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Chemical Property of (trans-1,4-diphenylcyclohexane)tricarbonylchromium

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Technology Process of (trans-1,4-diphenylcyclohexane)tricarbonylchromium

There total 1 articles about (trans-1,4-diphenylcyclohexane)tricarbonylchromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 10470-04-9
trans-1,4-diphenylcyclohexane

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 98859-22-4
(trans-1,4-diphenylcyclohexane)tricarbonylchromium

Guidance literature:: With α-picoline; In diethylene glycol; under N2; a mixt. of Cr-compd. and trans-1,4-diphenylcyclohexane in dry diglyme in the presence of 2-methylpyridine is refluxed until the evolution of gas ceases (6 h); the cooled soln. is filtered with the aid of Celite, freed of solvent and the residue is chromd. on silica gel, elution with light petroleum -benzene and crystn. from this solvent, elem. anal.;
DOI:10.1039/P19870000747

Reference yield: 32.0%

: 98859-22-4
(trans-1,4-diphenylcyclohexane)tricarbonylchromium

: 113031-50-8
(trans-1-(4''-acetylphenyl)-4-phenylcyclohexane)tricarbonylchromium

: 56359-32-1
trans-1,4-bis(4'-acetylphenyl)cyclohexane

Guidance literature:: With aluminium trichloride; acetyl chloride; In dichloromethane; Friedel-Crafts acetylation; anhydrous AlCl3-powder in CH2Cl2 is stirred at 0°C under N2, addn. of acetylchloride in CH2Cl2, stirring (30 min), Cr-compd. is added dropwise within 30 min (stirring, 0°C), further stirring (room temp., 5 h); mixt. is poured into ice-water, sepn. of the layers, the aq. layer is extd. with CH2Cl2, combined org. layers are washed (water, aq. NaHCO3), dried (Na2SO4), concd. (vac., 40-50°C),crystn. from benzene-light petroleum, elem. anal.;
DOI:10.1039/P19870000747