2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

Base Information

Chemical Name:2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid
CAS No.:127054-66-4
Molecular Formula:C₉H₉F₄O₅P
Molecular Weight:304.135
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

Chemical Property:

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Technology Process of 2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

There total 7 articles about 2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127054-63-1
2-(2,2,3,3-tetrafluoropropoxy)-2-oxobenzo-1,3,2λ⁵-dioxaphosphole

: 127054-66-4
2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

Guidance literature:: With air moisture; In acetonitrile; at 20 ℃; for 6h;

Reference yield:

: 88399-68-2
2-(2,2,3,3-tetrafluoropropoxy)-4,5-benzo-1,3,2-dioxaphospholane

: 127054-66-4
2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 3 d, r.t., 2) 120 deg C, 40 min; reaction with alkyl halides or alcohol

2: air moisture / acetonitrile / 6 h / 20 °C

With air moisture; In acetonitrile;

Reference yield:

: 127054-67-5
2,2-dibromo-2-(2,2,3,3-tetrafluoropropoxy)benzo-1,3,2λ⁵-dioxaphosphole

: 127054-66-4
2-hydroxyphenyl-2,2,3,3-tetrafluoropropylphosphoric acid

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃

2: 94 percent / NEt₃ / CH₂Cl₂ / 0.5 h / -40 °C

3: air moisture / acetonitrile / 6 h / 20 °C

With air moisture; triethylamine; In dichloromethane; acetonitrile;