cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione

Base Information

• Chemical Name: cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione
• CAS No.: 53976-01-5
• Molecular Formula: C₂₀H₁₈N₂O₂
• Molecular Weight: 318.375

Synonyms:

Chemical Property of cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione

Chemical Property:

Purity/Quality:

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Technology Process of cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione

There total 2 articles about cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-2-amino-3-(2'-ethyl-3'-phenylaziridino)-1,4-naphthoquinone (53975-91-0) → trans-1-phenyl-1-butene (1005-64-7) + 2-ethyl-3-phenyl-5,10-dihydrobenzoquinoxaline-5,10-dione (78742-09-3) + 2-(1-phenylpropyl)-1H-naphthoimidazole-4,9-dione (78742-13-9) + cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione (53976-01-5,78742-04-8,78742-05-9)

Guidance literature:

In xylene; for 2.5h; Further byproducts given; Heating;

Reference yield:

cis-2-amino-3-(2'-ethyl-3'-phenylaziridino)-1,4-naphthoquinone (53975-91-0) → trans-1-phenyl-1-butene (1005-64-7) + 2-ethyl-3-phenyl-5,10-dihydrobenzoquinoxaline-5,10-dione (78742-09-3) + 2-(1-phenylpropyl)-1H-naphthoimidazole-4,9-dione (78742-13-9) + trans-4H-2,3,5,6-tetrahydro-2-phenyl-3-ethyl-5-iminonaphtho<1,2-b>oxazin-6-one (78742-14-0,78742-15-1) + cis-4H-2,3,5,6-tetrahydro-2-phenyl-3-ethyl-5-iminonaphtho<1,2-b>oxazin-6-one (78742-14-0,78742-15-1) + cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione (53976-01-5,78742-04-8,78742-05-9)

Guidance literature:

In xylene; for 2.5h; Mechanism; Heating; other temp., other solvent, further products,;

Reference yield:

cis-2-ethyl-3-phenyl-1,2,3,4,5,10-hexahydrobenzoquinoxaline-5,10-dione (53976-01-5,78742-04-8,78742-05-9) → 2-ethyl-3-phenyl-1,2,5,10-tetrahydrobenzoquinoxaline-5,10-dione (78742-10-6)

Guidance literature:

With iron(III) chloride; In ethanol;

upstream raw materials:

cis-2-amino-3-(2'-ethyl-3'-phenylaziridino)-1,4-naphthoquinone

Downstream raw materials:

2-ethyl-3-phenyl-1,2,5,10-tetrahydrobenzoquinoxaline-5,10-dione

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