oxo hydroxo bis-benzhydroxamato vanadium (V)

Base Information

Chemical Name:oxo hydroxo bis-benzhydroxamato vanadium (V)
CAS No.:20274-24-2
Molecular Formula:C₁₄H₁₃N₂O₆V
Molecular Weight:356.209
Hs Code.:

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Chemical Property of oxo hydroxo bis-benzhydroxamato vanadium (V)

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Technology Process of oxo hydroxo bis-benzhydroxamato vanadium (V)

There total 2 articles about oxo hydroxo bis-benzhydroxamato vanadium (V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: ammonium vanadate(V)

: 495-18-1
Benzohydroxamic acid

: 20274-24-2
oxo hydroxo bis-benzhydroxamato vanadium (V)

Guidance literature:: In water; an aq. mixt. of benzohydroxamic acid and NH4VO3 is acidified to pH of 3-4 with diluted H2SO4; digestion on a water bath for 0.5 h;; ppt. is filtered off, washed with water and finally with ether and dried in vacuo: elem. anal.;;

Reference yield:

: ammonium vanadate(V)

: 20274-24-2
oxo hydroxo bis-benzhydroxamato vanadium (V)

Guidance literature:: With K-benzhydroxamate; In water; addition of H2SO4 to a solution of 0.4 g K-benzhydroxamate and 0.1 g NH4VO3 (to pH = 3);; precipitation; washing with water and drying in vacuum over CaCl2;;

Reference yield: 60.0%

: 20274-24-2
oxo hydroxo bis-benzhydroxamato vanadium (V)

: 19630-84-3
oxo methoxo bis-benzhydroxamato vanadium (V)

Guidance literature:: With CH₃OH; In methanol; V complex is refluxed in methanol for 2 h;; crystn. on cooling to 0°C; crystals are filtered off and dried over fused CaCl2;;