Technology Process of C28H36O5SSi
There total 3 articles about C28H36O5SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: manganese(IV) oxide / dichloromethane / 0.67 h / 20 °C / Inert atmosphere
2.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere
2.2: 12 h / -78 °C / Inert atmosphere
With
pyridine; manganese(IV) oxide;
In
dichloromethane;
DOI:10.1021/ja309905j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran / 1.67 h / -78 - 0 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.83 h / -78 °C / Inert atmosphere
3.1: manganese(IV) oxide / dichloromethane / 0.67 h / 20 °C / Inert atmosphere
4.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere
4.2: 12 h / -78 °C / Inert atmosphere
With
pyridine; manganese(IV) oxide; n-butyllithium; diisobutylaluminium hydride; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja309905j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.83 h / -78 °C / Inert atmosphere
2.1: manganese(IV) oxide / dichloromethane / 0.67 h / 20 °C / Inert atmosphere
3.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere
3.2: 12 h / -78 °C / Inert atmosphere
With
pyridine; manganese(IV) oxide; diisobutylaluminium hydride;
In
hexane; dichloromethane;
DOI:10.1021/ja309905j