[(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF₆

Base Information

• Chemical Name: [(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF₆
• CAS No.: 247565-13-5
• Molecular Formula: C₃₈H₃₇FeNPRu*F₆P
• Molecular Weight: 840.573
• Mol file: 247565-13-5.mol

Synonyms:

Chemical Property of [(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF₆

There total 1 articles about [(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

[(SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(CH3CN)]PF6 (247195-85-3) + phenylacetylene (536-74-3) → [(R/SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(=C=CHPh)]PF6 (247565-13-5,247195-95-5)

Guidance literature:

In dichloromethane; Ar-atmosphere; CO-atmosphere (2 min), stirring (room temp., 3 h), evapn.; CH2Cl2 addn., pptn. on Et2O addn.; elem. anal., isolated as mixture of diastereomers;

DOI:10.1021/om990307a

upstream raw materials:

[(SRu, Spl)-RuCp(2-(1-N,N-dimethylaminomethyl)-1-diphenylphosphino ferrocene)(CH₃CN)]PF₆

phenylacetylene