methyl (2S,3R)-2--3-methoxy-3-phenylpropanoate

Base Information

Chemical Name:methyl (2S*,3R*)-2--3-methoxy-3-phenylpropanoate
CAS No.:133379-85-8
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

methyl (2S*,3R*)-2-<propen-3-yl>-3-methoxy-3-phenylpropanoate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S*,3R*)-2--3-methoxy-3-phenylpropanoate

Chemical Property:

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Technology Process of methyl (2S*,3R*)-2--3-methoxy-3-phenylpropanoate

There total 11 articles about methyl (2S*,3R*)-2--3-methoxy-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24850-33-7
allyltributylstanane

: 93643-71-1,131846-31-6,133379-84-7
methyl (±)-anti-2-iodo-3-methoxy-3-phenylpropanoate

: 133379-85-8,142612-18-8,142612-19-9
methyl (2R*,3R*)-2--3-methoxy-3-phenylpropanoate

Guidance literature:: With triethyl borane; In hexane; dichloromethane; at -78 ℃; for 3h;
DOI:10.1021/ja9541241

Reference yield:

: 103-26-4,1754-62-7
Methyl cinnamate

: 133379-85-8,142612-18-8,142612-19-9
methyl (2R*,3R*)-2--3-methoxy-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / I₂, AgNO₃ / 6 h / Ambient temperature

2: Et₃B / CH₂Cl₂; hexane / 3 h / -78 °C

With triethyl borane; iodine; silver nitrate; In hexane; dichloromethane;
DOI:10.1021/ja9541241

Reference yield:

: 52742-05-9,52781-50-7,60456-13-5,64856-34-4,65091-58-9
methyl (+/-)-(2R,3R)-2-bromo-3-methoxy-3-phenylpropanoate

: 24850-33-7
allyltributylstanane

: 133379-85-8,142612-18-8,142612-19-9
methyl (2R*,3R*)-2--3-methoxy-3-phenylpropanoate

: 133379-85-8,142612-18-8,142612-19-9
methyl (2S*,3R*)-2--3-methoxy-3-phenylpropanoate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; at -78 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;
DOI:10.1021/jo00042a029