(3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Base Information

Chemical Name:(3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate
CAS No.:87530-82-3
Molecular Formula:C₃₀H₄₆O₃
Molecular Weight:454.693
Hs Code.:

(3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

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Chemical Property of (3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

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Technology Process of (3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

There total 1 articles about (3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2311-91-3
monoperoxyphthalic acid

: 4356-12-1
(22E)-3β-acetoxy-5α-ergosta-7,14,22-triene

: 87530-82-3
3β-acetoxy-5α-ergosta-8(14),22t-dien-15-one

: phthalic acid mono-(3β-acetoxy-15ξ-hydroxy-5α-ergosta-8(14),22t-dien-7ξ-yl ester)

Guidance literature:: DOI:10.1039/jr9540000052

Reference yield: 95.0%

: 87530-82-3
(3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

: 705926-28-9
(22E)-3β-hydroxyergosta-8(14),22-dien-15-one

Guidance literature:: With potassium carbonate; In methanol; water; for 1h; Heating;
DOI:10.1023/B:RUBI.0000015777.32627.7f

Reference yield:

: 87530-82-3
(3S,5S,9R,10S,13R,17R)-17-((2R,5R,E)-5,6-dimethylhept-3-en-2-yl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,9,10,11,12,13,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

: 87530-85-6
C₃₇H₅₃NO₅S

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine, hydroxylamine hydrochloride / methanol / 1 h / Heating

2: 1 g / pyridine / 16 h

With pyridine; hydroxylamine hydrochloride; In methanol;
DOI:10.1016/S0040-4020(01)91938-6