(2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

Base Information

• Chemical Name: (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol
• CAS No.: 55287-35-9
• Molecular Formula: C₂₅H₃₀O₁₁
• Molecular Weight: 506.507

Synonyms:

Chemical Property of (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

Chemical Property:

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MSDS Files:

Useful:

Technology Process of (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

There total 1 articles about (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (55287-35-9)

Guidance literature:

aus Pentaacetat 19, NaOMe/MeOH;

DOI:10.1016/S0008-6215(00)82369-1

Reference yield: 100.0%

benzyl chloride (100-44-7) + (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (55287-35-9,55287-36-0,87638-63-9) → Phenyl-O-(2,3-di-O-benzyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (87591-14-8,99746-02-8)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 2.5h; Heating;

Reference yield: 25.0%

benzyl chloride (100-44-7) + (2R,4aR,6R,7R,8R,8aS)-6-((2R,3S,4R,5R,6R)-4,5-Dihydroxy-2-hydroxymethyl-6-phenoxy-tetrahydro-pyran-3-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (55287-35-9,55287-36-0,87638-63-9) → Phenyl-O-(2,3-di-O-benzyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,6-di-O-benzyl-α-D-glucopyranosid (87591-15-9) + Phenyl-O-(2,3-di-O-benzyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid (87591-14-8,99746-02-8)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 7h; Heating;

Downstream raw materials:

Phenyl-O-(2,3-di-O-acetyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,6-di-O-acetyl-α-D-glucopyranosid

Phenyl-O-(2,3-di-O-benzyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,6-di-O-benzyl-α-D-glucopyranosid

Phenyl-O-(2,3-di-O-benzyl-4,6-O-benzyliden-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Phenyl-O-<4-(2-cyclohexenylamino)-4,6-didesoxy-α-D-glucopyranosyl>-(1->4)-α-D-glucopyranosid

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