N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide
CAS No.:1380602-67-4
Molecular Formula:C₈H₅BrF₃NO₂S
Molecular Weight:316.098
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

Chemical Property:

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Technology Process of N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

There total 2 articles about N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2905-24-0
3-Bromobenzenesulfonyl chloride

: 1380602-67-4
N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; sodium sulfite / tetrahydrofuran; water / 1 h / 75 °C / Inert atmosphere

2.1: thionyl chloride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / -78 - -20 °C / Inert atmosphere

3.2: 1.33 h / -78 °C / Inert atmosphere

With n-butyllithium; thionyl chloride; sodium hydrogencarbonate; sodium sulfite; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1021/ml3000935

Reference yield:

: 3-bromobenzenesulfinic acid

: 1380602-67-4
N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - -20 °C / Inert atmosphere

2.2: 1.33 h / -78 °C / Inert atmosphere

With n-butyllithium; thionyl chloride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ml3000935

Reference yield:

: 1380602-67-4
N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide

: 2491-20-5
L-alanine methyl ester hydrochloride

: C₁₂H₁₅BrN₂O₄S

: C₁₂H₁₅BrN₂O₄S

Guidance literature:: N-(3-bromophenylsulfinyl)-2,2,2-trifluoroacetamide; With N-chloro-succinimide; In acetonitrile; at -10 ℃; for 0.416667h; Inert atmosphere;

L-alanine methyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/ml3000935