C₂₅H₂₉NO

Base Information

• Chemical Name: C₂₅H₂₉NO
• CAS No.: 1453217-69-0
• Molecular Formula: C₂₅H₂₉NO
• Molecular Weight: 359.511
• Mol file: 1453217-69-0.mol

Synonyms:

Chemical Property of C₂₅H₂₉NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₉NO

There total 4 articles about C₂₅H₂₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H27NO (1453217-68-9) → C25H29NO (1453217-69-0)

Guidance literature:

C₂₅H₂₇NO; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 40 ℃; for 2h;

With water;

DOI:10.1055/s-0033-1339190

Reference yield:

C25H25NO → C25H29NO (1453217-69-0)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 40 °C

2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 40 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;

DOI:10.1055/s-0033-1339190

Reference yield:

(2-ethynylcyclohex-1-en-1-yl)(phenyl)methanone (436146-73-5) → C25H29NO (1453217-69-0)

Guidance literature:

Multi-step reaction with 3 steps

1: dirhodium tetraacetate / dichloromethane / 2 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 40 °C

3: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 40 °C

With dirhodium tetraacetate; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1055/s-0033-1339190

upstream raw materials:

C₂₅H₂₇NO

(2-ethynylcyclohex-1-en-1-yl)(phenyl)methanone

2,2-dimethyl-3-phenyl-2H-azirine