(C₆H₃(CH₂P(C₆H₁₁)2)2)NiH

Base Information

Chemical Name:(C₆H₃(CH₂P(C₆H₁₁)2)2)NiH
CAS No.:1160697-78-8
Molecular Formula:C₃₂H₅₂NiP₂
Molecular Weight:557.402
Hs Code.:

(C<sub>6</sub>H<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>11</sub>)2)2)NiH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₃(CH₂P(C₆H₁₁)2)2)NiH

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Technology Process of (C₆H₃(CH₂P(C₆H₁₁)2)2)NiH

There total 4 articles about (C₆H₃(CH₂P(C₆H₁₁)2)2)NiH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1160697-77-7
(C₆H₃(CH₂P(C₆H₁₁)2)2)NiCl

: 22560-16-3
lithium triethylborohydride

: 1160697-78-8
(C₆H₃(CH₂P(C₆H₁₁)2)2)NiH

Guidance literature:: In tetrahydrofuran; toluene; under Ar; Ni complex dissolved in toluene; cooled to 0°C (ice bath); soln. of LiEt3BH in THF added dropwise; warmed to room temp.; stirred overnight; volatiles removed under vac.; extd. in pentane; filtered; concd.; crystd. at -35°C; elem. anal.;
DOI:10.1021/ic8020194