2-triphenylphosphoranylideneaminomethylbenzimidazole

Base Information

• Chemical Name: 2-triphenylphosphoranylideneaminomethylbenzimidazole
• CAS No.: 123500-00-5
• Molecular Formula: C₂₆H₂₂N₃P
• Molecular Weight: 407.455

Synonyms:

Chemical Property of 2-triphenylphosphoranylideneaminomethylbenzimidazole

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-triphenylphosphoranylideneaminomethylbenzimidazole

There total 1 articles about 2-triphenylphosphoranylideneaminomethylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

triphenylphosphine (603-35-0) + 2-(azidomethyl)-1H-benzo[d]imidazole (66894-26-6) → 2-triphenylphosphoranylideneaminomethylbenzimidazole (123500-00-5)

Guidance literature:

In chloroform; benzene; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)80047-8

Reference yield: 83.0%

phenyl isocyanate (103-71-9) + 2-triphenylphosphoranylideneaminomethylbenzimidazole (123500-00-5) → 1-phenylimino-2-phenylcarbamoyl-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole (123500-01-6)

Guidance literature:

In benzene; for 5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)80047-8

Reference yield: 64.0%

p-Tolylisocyanate (622-58-2,374675-64-6) + 2-triphenylphosphoranylideneaminomethylbenzimidazole (123500-00-5) → 1-(p-tolylimino)-2-(p-tolylcarbamoyl)-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole (123500-02-7)

Guidance literature:

In benzene; for 5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)80047-8

upstream raw materials:

triphenylphosphine

2-(azidomethyl)-1H-benzo[d]imidazole

Downstream raw materials:

1-(m-tolylimino)-2-(m-tolylcarbamoyl)-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole

1-(p-chlorophenylimino)-2-(p-chlorophenylcarbamoyl)-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole

1-phenylimino-2-phenylcarbamoyl-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole

1-(p-tolylimino)-2-(p-tolylcarbamoyl)-2,3-dihydro-1H-imidazo<1,5-a>benzimidazole

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