cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰

Base Information

• Chemical Name: cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰
• CAS No.: 1173986-58-7
• Molecular Formula: C₁₁₀H₁₂₇Cl₄N₁₅O₂₂
• Molecular Weight: 2153.12

Synonyms:

Chemical Property of cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰

There total 1 articles about cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-Leu-Thr(Bzl)-Dab(2-ClZ)-Dab-Dab(2-ClZ)-D-Phe-Leu-Dab(2-ClZ)-Dab(2-ClZ)-Thr(BzL)-OH (1173986-46-3) → cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab4 and α-COOH of Thr10 (1173986-58-7)

Guidance literature:

With 4-methyl-morpholine; diphenyl phosphoryl azide; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 4 ℃; Cooling with ice;

DOI:10.1248/cpb.57.332

Reference yield:

cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab4 and α-COOH of Thr10 (1173986-58-7) → cyclic Leu-Thr-Dab-Dab-Dab-D-Phe-Leu-Dab-Dab-Thr, containing amide bond between γ-NH2 of Dab4 and α-COOH of Thr10 (873440-52-9)

Guidance literature:

cyclic Fmoc-Leu-Thr(Bzl)-Dab(2-CIZ)-Dab-Dab(2-CIZ)-D-Phe-Leu-Dab(2-CIZ)-Dab(2-CIZ)-Thr(Bzl), containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰; With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

With hydrogen fluoride; methoxybenzene; for 1h; Cooling with ice;

DOI:10.1248/cpb.57.332

upstream raw materials:

Fmoc-Leu-Thr(Bzl)-Dab(2-ClZ)-Dab-Dab(2-ClZ)-D-Phe-Leu-Dab(2-ClZ)-Dab(2-ClZ)-Thr(BzL)-OH

Downstream raw materials:

cyclic Leu-Thr-Dab-Dab-Dab-D-Phe-Leu-Dab-Dab-Thr, containing amide bond between γ-NH2 of Dab⁴ and α-COOH of Thr¹⁰

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