C₄₁H₇₇NO₇Si₃

Base Information

Chemical Name:C₄₁H₇₇NO₇Si₃
CAS No.:1355616-38-4
Molecular Formula:C₄₁H₇₇NO₇Si₃
Molecular Weight:780.321
Hs Code.:

C<sub>41</sub>H<sub>77</sub>NO<sub>7</sub>Si<sub>3</sub>

Synonyms:

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Chemical Property of C₄₁H₇₇NO₇Si₃

Chemical Property:

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Technology Process of C₄₁H₇₇NO₇Si₃

There total 12 articles about C₄₁H₇₇NO₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355616-47-5
C₃₅H₆₃NO₇Si₂

: 69739-34-0
t-butyldimethylsiyl triflate

: 1355616-38-4
C₄₁H₇₇NO₇Si₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ml200254h

Reference yield:

: 1254369-08-8
C₁₆H₂₂O₃

: 1355616-38-4
C₄₁H₇₇NO₇Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium osmate; K₃Fe(CN)6; (DHQD)2PHAL; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 36 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -45 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

7.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / ethanol

9.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

9.2: -78 - 20 °C / Inert atmosphere

10.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 0 °C / Inert atmosphere

10.2: -78 - 0 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; potassium osmate; methanesulfonamide; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; K₃Fe(CN)6; (DHQD)2PHAL; hydrogen; potassium carbonate; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Sharpless dihydroxylation / 9.1: Swern oxidation / 9.2: Swern oxidation;
DOI:10.1021/ml200254h

Reference yield:

: 1355616-31-7
C₁₅H₂₀O₄

: 1355616-38-4
C₄₁H₇₇NO₇Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

3.2: 2 h / -78 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -45 °C / Inert atmosphere

5.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

6.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

8.2: -78 - 20 °C / Inert atmosphere

9.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 0 °C / Inert atmosphere

9.2: -78 - 0 °C / Inert atmosphere

10.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; 8.1: Swern oxidation / 8.2: Swern oxidation;
DOI:10.1021/ml200254h