(9E)-(7-13C)-β-ionylideneacetaldehyde

Base Information

• Chemical Name: (9E)-(7-13C)-β-ionylideneacetaldehyde
• CAS No.: 100187-36-8
• Molecular Formula: C₁₅H₂₂O
• Molecular Weight: 219.328
• Mol file: 100187-36-8.mol

Synonyms:

Chemical Property of (9E)-(7-13C)-β-ionylideneacetaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (9E)-(7-13C)-β-ionylideneacetaldehyde

There total 3 articles about (9E)-(7-13C)-β-ionylideneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12(13)CH20O → (9E)-(7-13C)-β-ionylideneacetaldehyde (100187-36-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / 96percent H₂SO₄ / nitromethane / 0 - 10 °C

2: 1) NaH

3: 1) DIBAL, 2) H₂O

With sulfuric acid; water; sodium hydride; diisobutylaluminium hydride; In nitromethane;

Reference yield:

(9E)-(7-13C)-β-ionylideneacetonitrile (105176-07-6) → (9E)-(7-13C)-β-ionylideneacetaldehyde (100187-36-8)

Guidance literature:

With water; diisobutylaluminium hydride; Multistep reaction;

Reference yield:

(7-13C)-γ-ionone (100187-34-6) → (9E)-(7-13C)-β-ionylideneacetaldehyde (100187-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaH

2: 1) DIBAL, 2) H₂O

With water; sodium hydride; diisobutylaluminium hydride;

upstream raw materials:

(9E)-(7-13C)-β-ionylideneacetonitrile

(7-13C)-γ-ionone

Refernces