<2R^*-<2α(S^*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine

Base Information

• Chemical Name: <2R^*-<2α(S^*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzo
• Molecular Formula: C₄₂H₄₇N₃O₃
• Molecular Weight: 641.853

Synonyms:

Chemical Property of <2R^*-<2α(S^*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

There total 10 articles about <2R^*-<2α(S^*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine (74059-19-1,106550-20-3) → <2R*-<2α(R*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine (74059-20-4,74111-72-1,106622-54-2,106622-55-3) + <2R*-<2α(S*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine (74059-20-4,74111-72-1,106622-54-2,106622-55-3)

Guidance literature:

With hydrogen; 3,4-methylenedioxymethamphetamine; In 1,4-dioxane; at 29 ℃; for 0.666667h;

DOI:10.1248/cpb.33.3724

Reference yield: 29.0%

(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine (74059-19-1,106550-20-3) → <2R*-<2α(R*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine (74059-20-4,74111-72-1,106622-54-2,106622-55-3) + <2R*-<2α(S*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine (74059-20-4,74111-72-1,106622-54-2,106622-55-3)

Guidance literature:

With hydrogen; 3,4-methylenedioxymethamphetamine; In 1,4-dioxane; at 29 ℃; for 0.666667h;

DOI:10.1248/cpb.33.3724

Reference yield:

(+/-)-9-benzyloxy-N-<2-(5-benzyloxy-1H-indol-3-yl)ethyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine-2β-acetamide (74059-18-0,106622-53-1) → <2R*-<2α(R*),3β,11bβ>>-9-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-10-methoxy-2H-benzoquinolizine (74059-20-4,74111-72-1,106622-54-2,106622-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / POCl₃ / toluene / 2.5 h / Heating

2: 54 percent / H₂ / PtO₂*H₂O / dioxane / 0.67 h / 29 °C / 760 Torr

With hydrogen; trichlorophosphate; platinum(IV) oxide; In 1,4-dioxane; toluene;

upstream raw materials:

(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine

5-benzyloxytryptamine

(+/-)-9-benzyloxy-N-<2-(5-benzyloxy-1H-indol-3-yl)ethyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine-2β-acetamide

((3S,4S)-6-Ethoxy-3-ethyl-2,3,4,5-tetrahydro-pyridin-4-yl)-acetic acid ethyl ester

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