1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole

Base Information

• Chemical Name: 1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole
• CAS No.: 1415305-95-1
• Molecular Formula: C₇₆H₈₅N₃O₁₇P₂Si
• Molecular Weight: 1402.55

Synonyms:

Chemical Property of 1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole

Chemical Property:

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Technology Process of 1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole

There total 1 articles about 1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C53H59O8PSi (1415305-91-7) + azido-2,3-O-acetyl-5-O-(dibenzylphosphate)-β-D-ribofuranoside (1415305-68-8) → 1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole (1415305-95-1)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 40 ℃; for 8h;

DOI:10.1039/c2ob26577j

Reference yield:

1-[2,3-di-O-acetyl-5-O-(diphenylphosphatyl)-β-D-ribofuranosyl]-4-methylenoxy-[5-(3S,4R,5R)-3,4-di-O-benzyl-6-O-(dibenzylphosphatyl)-1-O-(tert-butyldiphenylsilyl)-hexanyl]-1H-1,2,3-triazole (1415305-95-1) → C60H67N3O17P2

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran;

DOI:10.1039/c2ob26577j

upstream raw materials:

C₅₃H₅₉O₈PSi

azido-2,3-O-acetyl-5-O-(dibenzylphosphate)-β-D-ribofuranoside

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