4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

Base Information

Chemical Name:4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine
CAS No.:1565870-81-6
Molecular Formula:C₁₂H₈ClN₃
Molecular Weight:229.669
Hs Code.:

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Chemical Property of 4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

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Technology Process of 4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

There total 6 articles about 4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1565870-80-5
3-phenyl-3H-imidazo[4,5-c]pyridine 5-oxide

: 1565870-81-6
4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

Guidance literature:: With trichlorophosphate; at 120 ℃; for 2h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/jo500064j

Reference yield:

: 1565870-60-1
C₁₁H₉ClN₂

: 1565870-81-6
4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / tert-butyl alcohol / 6.5 h / 110 °C / Schlenk technique; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 45 °C / Schlenk technique; Inert atmosphere

3: trichlorophosphate / 2 h / 120 °C / Schlenk technique; Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In chloroform; tert-butyl alcohol;
DOI:10.1021/jo500064j

Reference yield:

: 1565870-83-8
C₁₆H₁₇ClN₂O₂

: 1565870-81-6
4-chloro-3-phenyl-3H-imidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: potassium phosphate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / tert-butyl alcohol / 6.5 h / 110 °C / Schlenk technique; Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 45 °C / Schlenk technique; Inert atmosphere

4: trichlorophosphate / 2 h / 120 °C / Schlenk technique; Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trichlorophosphate; In dichloromethane; chloroform; tert-butyl alcohol;
DOI:10.1021/jo500064j