nido-Ph₂C₂B₄H₆

Base Information

Chemical Name:nido-Ph₂C₂B₄H₆
CAS No.:110719-62-5
Molecular Formula:C₁₄H₁₆B₄
Molecular Weight:227.525
Hs Code.:

nido-Ph<sub>2</sub>C<sub>2</sub>B<sub>4</sub>H<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of nido-Ph₂C₂B₄H₆

Chemical Property:

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Technology Process of nido-Ph₂C₂B₄H₆

There total 2 articles about nido-Ph₂C₂B₄H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 19624-22-7
pentaborane⁽⁹⁾

: 501-65-5
diphenyl acetylene

: 110719-62-5
nido-Ph₂C₂B₄H₆

Guidance literature:: In neat (no solvent); heated at 180°C in a steel cylinder;
DOI:10.1351/pac198759070847

Reference yield:

: 19624-22-7
pentaborane⁽⁹⁾

: 501-65-5
diphenyl acetylene

: ((C₆H₅)2C₂)5(C₆H₅)2C₂B₅H₇

: 110719-62-5
nido-Ph₂C₂B₄H₆

: ((C₆H₅)2C₂)4(C₆H₅)2C₂B₅H₇

: (C₆H₅)4C₄B₄H₄

Guidance literature:: In hexane; B5H9 condensed into mixt. of Ph2C2 and n-hexane at -196 ° C in vacuo in a steel cylinder; cylinder closed and heated to 180 ° C for 3 days; cooling; evapn. with warming; addn. of n-hexane at -196 ° C, cylinder filled with Ar;; extn. with benzene, CH2Cl2 and acetone; dried extract chromd. (silica gel/n-hexane- column, benzene); evapn., residue distd. and heated to 50 ° C under vac.; distillate chromd. (TLC, silica, n-hexane); exact mass; UV- spectrum;;