C₁₂H₁₅BrO₄

Base Information

Chemical Name:C₁₂H₁₅BrO₄
CAS No.:1433061-88-1
Molecular Formula:C₁₂H₁₅BrO₄
Molecular Weight:303.153
Hs Code.:

C<sub>12</sub>H<sub>15</sub>BrO<sub>4</sub>

Synonyms:

Suppliers and Price of C₁₂H₁₅BrO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₅BrO₄

Chemical Property:

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Technology Process of C₁₂H₁₅BrO₄

There total 5 articles about C₁₂H₁₅BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1433061-58-5
C₁₈H₂₉BrO₄Si

: 1433061-88-1
C₁₂H₁₅BrO₄

Guidance literature:: With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja4018122

Reference yield:

: 95-56-7
2-hydroxybromobenzene

: 1433061-88-1
C₁₂H₁₅BrO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

1.2: 3 h / Reflux

2.1: sodium tetrahydroborate / methanol / 0 °C

3.1: 1H-imidazole / dichloromethane / 0 - 20 °C

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

5.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 20 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; di-isopropyl azodicarboxylate; pyridine hydrogenfluoride; triethylamine; triphenylphosphine; magnesium chloride; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja4018122

Reference yield:

: 1433061-28-9
C₁₃H₂₁BrO₂Si

: 1433061-88-1
C₁₂H₁₅BrO₄

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; pyridine hydrogenfluoride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/ja4018122