Technology Process of C19H30O3Si
There total 5 articles about C19H30O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium; boron trifluoride diethyl etherate;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 3h;
DOI:10.1055/s-0033-1340164
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 12 h / 0 - 20 °C
2: triphenylphosphine / dichloromethane / 3 h / 0 - 20 °C
3: potassium carbonate; potassium hexacyanoferrate(III); methanesulfonamide; potassium osmate(VI) dihydrate; hydroquinine (anthraquinone-1,4-diyl) diether / water; tert-butyl alcohol / 3.5 h / 0 °C
4: lithium diisopropyl amide / tetrahydrofuran / 3 h / -10 °C
5: n-butyllithium; boron trifluoride diethyl etherate / tetrahydrofuran / 3 h / -78 - 20 °C
With
potassium osmate(VI) dihydrate; n-butyllithium; hydroquinine (anthraquinone-1,4-diyl) diether; methanesulfonamide; boron trifluoride diethyl etherate; potassium carbonate; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hexacyanoferrate(III); lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
3: |Sharpless Dihydroxylation;
DOI:10.1055/s-0033-1340164
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -10 °C
2: n-butyllithium; boron trifluoride diethyl etherate / tetrahydrofuran / 3 h / -78 - 20 °C
With
n-butyllithium; boron trifluoride diethyl etherate; lithium diisopropyl amide;
In
tetrahydrofuran;
DOI:10.1055/s-0033-1340164
