CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

Base Information

Chemical Name:CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))
CAS No.:1313752-10-1
Molecular Formula:C₁₉H₂₂BCoO₂S₂
Molecular Weight:416.319
Hs Code.:

CpCo(S<sub>2</sub>C<sub>2</sub>H(p-C<sub>6</sub>H<sub>4</sub>(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

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Suppliers and Price of CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

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Technology Process of CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

There total 1 articles about CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane))) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1313752-09-8
CpCo(S₂C₂H)(p-C₆H₄Br)

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1313752-10-1
CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

: 1313752-11-2
CpCo(S₂C₂(p-C₆H₄Br)(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With NEt₃; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; under Ar, Schlenk technique; Co complex and Bpin-H reacted in presence of Pd complex in NEt3 and 1,4-dioxane; react. mixt. eated at 80°C for 24 h; volatiles removed in vac; mixt. separated by HPLC; recrystd. by CH2Cl2/n-hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2011.04.014

Reference yield: 24.0%

: 109-04-6
2-bromo-pyridine

: 1313752-10-1
CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

: (η5-cyclopentadienyl)(1-phenyl-1,2-ethenedithiolato)cobalt(III)

: 1313752-14-5
CpCo(S₂C₂H(p-C₆H₄(2-Py)))

Guidance literature:: With Na₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; under Ar, using Schlenk technique; Co complex, 2-bromopyridine, Pd(PPh3)4, aq. Na2CO3 reacted in refluxing THF for 4 h; volatiles removed in vac.; separated by HPLC; elem. anal.;
DOI:10.1016/j.jorganchem.2011.04.014

Reference yield: 10.0%

: 1564-64-3
9-Bromoanthracene

: 1313752-10-1
CpCo(S₂C₂H(p-C₆H₄(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)))

: (η5-cyclopentadienyl)(1-phenyl-1,2-ethenedithiolato)cobalt(III)

: 1313752-15-6
CpCo(S₂C₂H(p-C₆H₄(9-Anth)))

Guidance literature:: With Na₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; under Ar, using Schlenk technique; Co complex, 9-bromoanthracene, Pd(PPh3)4, aq. Na2CO3 reacted in refluxing THF for 4 h; volatiles removed in vac.; separated by HPLC; elem. anal.;
DOI:10.1016/j.jorganchem.2011.04.014