1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane

Base Information

• Chemical Name: 1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane
• CAS No.: 127794-24-5
• Molecular Formula: C₆₁H₉₄Ge₂
• Molecular Weight: 972.597
• Mol file: 127794-24-5.mol

Synonyms:

Chemical Property of 1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane

There total 1 articles about 1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + di(2,4,6-triisopropylphenyl)bis(trimethylsilyl)germane (115534-71-9) → 1,1,2,2-tetrakis(2,4,6-triisopropylphenyl)digermirane (127794-24-5)

Guidance literature:

In diethyl ether; pentane; byproducts: N2; Irradiation (UV/VIS); Ar-atmosphere; irradiation of germane solution (125 W low pressure Hg lamp, room temp., 23 h), addn. to Et2O soln. of CH2N2 (-78°C), warming to room temp.; evapn., chromy. (SiO2, hexane); elem. anal.;

DOI:10.1021/om00157a014

upstream raw materials:

diazomethane

di(2,4,6-triisopropylphenyl)bis(trimethylsilyl)germane