methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

Base Information

Chemical Name:methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside
CAS No.:86964-38-7
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:

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Chemical Property of methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

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Technology Process of methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

There total 1 articles about methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85230-78-0
methyl-3-O-benzyl-2,6-didesoxy-β-L-lyxo-hexopyranoside

: 86964-38-7
methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

Guidance literature:: acetylation;
DOI:10.1039/c39830000305

Reference yield:

: 86964-38-7
methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

: N-{(2S,3S,4S,6R)-6-Benzyloxy-3-[(2S,4S,5R,6S)-4-benzyloxy-5-((2S,5R,6S)-5-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-2-yloxy]-2-methyl-tetrahydro-pyran-4-yl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) bromotrimethylsilane, 2.) HgBr₂, HgO / 1.) benzene, r.t., 2.) CH₂Cl₂, 15 min 0 deg C then 1 h r.t.

2: NaOMe / methanol

3: 68 percent / N-iodosuccinimide / acetonitrile / 1 h / 0 °C

4: H₂, Et₃N / Pd-C / ethanol

With N-iodo-succinimide; trimethylsilyl bromide; hydrogen; sodium methylate; triethylamine; mercury dibromide; mercury(II) oxide; palladium on activated charcoal; In methanol; ethanol; acetonitrile;
DOI:10.1039/c39830000305

Reference yield:

: 86964-38-7
methyl 3-O-benzyl-4-O-acetyl-2-deoxy-β-L-fucoside

: Acetic acid (2S,3R,6S)-6-{(2S,3R,4S,6S)-4-benzyloxy-6-[(2S,3S,4S,6R)-6-benzyloxy-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yloxy]-2-methyl-tetrahydro-pyran-3-yloxy}-2-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) bromotrimethylsilane, 2.) HgBr₂, HgO / 1.) benzene, r.t., 2.) CH₂Cl₂, 15 min 0 deg C then 1 h r.t.

2: NaOMe / methanol

3: 68 percent / N-iodosuccinimide / acetonitrile / 1 h / 0 °C

4: H₂, Et₃N / Pd-C / ethanol

With N-iodo-succinimide; trimethylsilyl bromide; hydrogen; sodium methylate; triethylamine; mercury dibromide; mercury(II) oxide; palladium on activated charcoal; In methanol; ethanol; acetonitrile;
DOI:10.1039/c39830000305