(C₅Me₅)Fe(CO)2SiBrMePh

Base Information

Chemical Name:(C₅Me₅)Fe(CO)2SiBrMePh
CAS No.:745811-89-6
Molecular Formula:C₁₉H₂₃BrFeO₂Si
Molecular Weight:447.227
Hs Code.:

(C<sub>5</sub>Me<sub>5</sub>)Fe(CO)2SiBrMePh

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Chemical Property of (C₅Me₅)Fe(CO)2SiBrMePh

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Technology Process of (C₅Me₅)Fe(CO)2SiBrMePh

There total 1 articles about (C₅Me₅)Fe(CO)2SiBrMePh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 745811-87-4
(C₅Me₅)Fe(CO)2SiMe₂Ph

: 10294-33-4
boron tribromide

: 745811-89-6
(C₅Me₅)Fe(CO)2SiBrMePh

Guidance literature:: In toluene; byproducts: MeBBr2; under inert atm.; BBr3 was added dropwise to a toluene soln. of Fe-complex at room temp., the mixt. was stirred at room temp. for 6 h; evapd., hexane was added, filtd., filtrate evapd.; elem. anal.;
DOI:10.1021/om049762j

Reference yield:

: 745811-89-6
(C₅Me₅)Fe(CO)2SiBrMePh

: 10294-33-4
boron tribromide

: 745811-92-1
(C₅Me₅)Fe(CO)2SiBr₂Ph

Guidance literature:: In benzene-d6; byproducts: MeBBr3; BBr3 (1.2 equiv.) was added to a C6D6 soln. of Fe-complex in a Pyrex NMRtube at room temp., the NMR tube was degassed and sealed, the soln. was heated at 50°C for 96 h; the reaction was monitored by (1) NMR s pectroscopy; not isolated; detd. by (1)H NMR spectroscopy;
DOI:10.1021/om049762j