methyltris(diphenyltrimethylstannylphosphine)cobalt

Base Information

Chemical Name:methyltris(diphenyltrimethylstannylphosphine)cobalt
CAS No.:107604-05-7
Molecular Formula:C₄₆H₆₀CoP₃Sn₃
Molecular Weight:1121.03
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Chemical Property of methyltris(diphenyltrimethylstannylphosphine)cobalt

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Technology Process of methyltris(diphenyltrimethylstannylphosphine)cobalt

There total 1 articles about methyltris(diphenyltrimethylstannylphosphine)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: cobalt(III) acetylacetonate

: 1213-51-0
(trimethylstannyl)diphenylphosphine

: 107604-05-7
methyltris(diphenyltrimethylstannylphosphine)cobalt

Guidance literature:: With trimethylaluminum; In diethyl ether; pentane; (Ar); addn. of a soln. of trimethylaluminum in pentane to a mixt. of cobalt acetylacetonate and diphenyltrimethylstannylphosphine in diethyl ether at -35°C, stirring for 2 h, then warming to 0°C (formation of a brown ppt.); evapn. of some of the solvent, addn. of pentane, filtration of ppt., washing (pentane, -30°C), drying (vac., room temp.); elem. anal.;
DOI:10.1016/S0022-328X(00)99664-5