C₂₅H₃₆F₂N₂O₄

Base Information

Chemical Name:C₂₅H₃₆F₂N₂O₄
CAS No.:1292321-51-7
Molecular Formula:C₂₅H₃₆F₂N₂O₄
Molecular Weight:466.569
Hs Code.:

C<sub>25</sub>H<sub>36</sub>F<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₅H₃₆F₂N₂O₄

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Technology Process of C₂₅H₃₆F₂N₂O₄

There total 13 articles about C₂₅H₃₆F₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1292321-50-6
C₂₆H₃₈F₂N₂O₄

: 1292321-51-7
C₂₅H₃₆F₂N₂O₄

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 75 ℃; for 3h;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₁₄H₂₀Cl₃NO₅

: 1292321-51-7
C₂₅H₃₆F₂N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: hydrogenchloride / methanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol

9: Decaborane / methanol / 20 °C

10: water; lithium hydroxide / tetrahydrofuran; methanol / 3 h / 75 °C

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; Decaborane; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-47-1
C₂₉H₃₄F₂N₂O₅

: 1292321-51-7
C₂₅H₃₆F₂N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / methanol / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

5: chloro-trimethyl-silane / dichloromethane / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethanol

7: Decaborane / methanol / 20 °C

8: water; lithium hydroxide / tetrahydrofuran; methanol / 3 h / 75 °C

With hydrogenchloride; chloro-trimethyl-silane; Decaborane; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060