4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide

Base Information

Chemical Name:4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide
CAS No.:15362-61-5
Molecular Formula:C₁₂H₁₁ClN₂O₂S
Molecular Weight:282.751
Hs Code.:
DSSTox Substance ID:DTXSID701185329

Synonyms:4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide;DTXSID701185329;15362-61-5

Suppliers and Price of 4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:282.0229765
Heavy Atom Count:18
Complexity:467

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C=CC(=NS(=O)(=O)C2=CC=C(C=C2)Cl)C=C1

Technology Process of 4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide

There total 5 articles about 4-Chloro-N-(1-methyl-4(1H)-pyridinylidene)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 126957-66-2
N-(p-Chlorphenylsulfonyl)-S-(1-methyl-4-pyridyliden)sulfimid

: 15362-61-5
N-(1-Methyl-4-pyridyliden)-p-chlorbenzolsulfonamid

Guidance literature:: at 201 ℃; for 0.25h; in vacuum;

Reference yield: 43.0%

: 126957-80-0
N,N'-Bis(p-chlorphenylsulfonyl)-S-(1-methyl-4-pyridinio)sulfodiimidat

: 15362-61-5
N-(1-Methyl-4-pyridyliden)-p-chlorbenzolsulfonamid

Guidance literature:: at 193 ℃; for 0.25h; in vacuum;

Reference yield:

: 15592-05-9
4-chloro-1-methylpyridin-1-ium iodide

: 15362-61-5
N-(1-Methyl-4-pyridyliden)-p-chlorbenzolsulfonamid

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / sodium sulfide*9H₂O / ethanol / 6 h / 60 °C

2: 79 percent / ethanol; CHCl₃ / 1.5 h / 0 °C

3: 56 percent / ethanol; CHCl₃ / 3 h / Ambient temperature

4: 43 percent / 0.25 h / 193 °C / in vacuum

With sodium sulfide; In ethanol; chloroform;