C₂₉H₂₆F₃N₃O₅

Base Information

Chemical Name:C₂₉H₂₆F₃N₃O₅
CAS No.:1307811-60-4
Molecular Formula:C₂₉H₂₆F₃N₃O₅
Molecular Weight:553.538
Hs Code.:

C<sub>29</sub>H<sub>26</sub>F<sub>3</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₉H₂₆F₃N₃O₅

Chemical Property:

Purity/Quality:

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Technology Process of C₂₉H₂₆F₃N₃O₅

There total 13 articles about C₂₉H₂₆F₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3470-50-6
6-Hydroxy-1-tetralone

: 1307811-61-5
C₂₉H₂₆F₃N₃O₅

: 1307811-60-4
C₂₉H₂₆F₃N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / 4 h / 0 - 20 °C

2.1: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

3.1: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

4.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

4.2: 1.17 h / 0 °C

4.3: 3 h / 110 °C / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

6.1: lithium perchlorate / 1-methyl-pyrrolidin-2-one / 71.5 h / 20 - 100 °C / Sealed vial

7.1: hydrogenchloride / acetonitrile; water / 2 h / 60 °C

8.1: CHIRALPAK_.(R). AD-H column / isopropyl alcohol; diethylamine; carbon dioxide

With pyridine; hydrogenchloride; n-butyllithium; hydroxylamine hydrochloride; sodium acetate; lithium perchlorate; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; hexane; dichloromethane; carbon dioxide; water; diethylamine; isopropyl alcohol; acetonitrile;

Reference yield:

: (3S)-1-(2-hydroxy-2-(3-(5-phenyl-4-(trifluoromethyl)isoxazol-3-yl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-yl)ethyl)piperidine-3-carboxylic acid hydrochloric acid

: 1307811-61-5
C₂₉H₂₆F₃N₃O₅

: 1307811-60-4
C₂₉H₂₆F₃N₃O₅

Guidance literature:: With CHIRALPAK AD-H column; In carbon dioxide; diethylamine; isopropyl alcohol; Purification / work up;

Reference yield:

: 144464-64-2
5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl trifluoromethanesulfonate

: 1307811-61-5
C₂₉H₂₆F₃N₃O₅

: 1307811-60-4
C₂₉H₂₆F₃N₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

2.1: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

3.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

3.2: 1.17 h / 0 °C

3.3: 3 h / 110 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

5.1: lithium perchlorate / 1-methyl-pyrrolidin-2-one / 71.5 h / 20 - 100 °C / Sealed vial

6.1: hydrogenchloride / acetonitrile; water / 2 h / 60 °C

7.1: CHIRALPAK_.(R). AD-H column / isopropyl alcohol; diethylamine; carbon dioxide

With hydrogenchloride; n-butyllithium; hydroxylamine hydrochloride; sodium acetate; lithium perchlorate; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; hexane; dichloromethane; carbon dioxide; water; diethylamine; isopropyl alcohol; acetonitrile;