Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester

Base Information

• Chemical Name: Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester
• CAS No.: 122600-22-0
• Molecular Formula: C₂₄H₃₈N₂O₆P₂S₄
• Molecular Weight: 640.787
• Mol file: 122600-22-0.mol

Synonyms:

Chemical Property of Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester

There total 2 articles about Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-(chloroacetyl)-2-(2-chloro-N-phenylacetamido)-1,4,5,6-tetrahydropyridine (122600-31-1) + potassium O,O-diethyldithiophosphate (3454-66-8) → Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester (122600-22-0)

Guidance literature:

In acetonitrile; Ambient temperature;

Reference yield:

2-(phenylamino)-3,4,5,6-tetrahydropyridine (67997-72-2) → Dithiophosphoric acid S-[({1-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-diethyl ester (122600-22-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / -20 - -10 °C

2: 70 percent / acetonitrile / Ambient temperature

In acetonitrile;

upstream raw materials:

1-(chloroacetyl)-2-(2-chloro-N-phenylacetamido)-1,4,5,6-tetrahydropyridine

potassium O,O-diethyldithiophosphate

2-(phenylamino)-3,4,5,6-tetrahydropyridine