Technology Process of C47H61NO5S2Si
There total 5 articles about C47H61NO5S2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: camphor-10-sulfonic acid / dichloromethane / 0 °C
2: 1H-imidazole / dichloromethane
3: diisobutylaluminium hydride / dichloromethane / -15 °C
4: Dess-Martin periodane; sodium hydrogencarbonate / 0 °C
5: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C
With
1H-imidazole; camphor-10-sulfonic acid; titanium tetrachloride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; (-)-sparteine;
In
dichloromethane;
DOI:10.1016/j.tetlet.2013.04.023
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dess-Martin periodane; sodium hydrogencarbonate / 0 °C
2: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C
With
titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; (-)-sparteine;
In
dichloromethane;
DOI:10.1016/j.tetlet.2013.04.023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / dichloromethane
2: diisobutylaluminium hydride / dichloromethane / -15 °C
3: Dess-Martin periodane; sodium hydrogencarbonate / 0 °C
4: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C
With
1H-imidazole; titanium tetrachloride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; (-)-sparteine;
In
dichloromethane;
DOI:10.1016/j.tetlet.2013.04.023