1-nitro-2,4,6-tricyclohexylbenzene

Base Information

• Chemical Name: 1-nitro-2,4,6-tricyclohexylbenzene
• CAS No.: 40049-67-0
• Molecular Formula: C₂₄H₃₅NO₂
• Molecular Weight: 369.547

Synonyms:

Chemical Property of 1-nitro-2,4,6-tricyclohexylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-nitro-2,4,6-tricyclohexylbenzene

There total 4 articles about 1-nitro-2,4,6-tricyclohexylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1,3,5-tricyclohexylbenzene (7325-14-6) → 1-nitro-2,4,6-tricyclohexylbenzene (40049-67-0)

Guidance literature:

With nitric acid; acetic anhydride; acetic acid; at 0 - 5 ℃; for 6h;

DOI:10.1002/ejic.201402830

Reference yield:

1-bromocyclohexane (108-85-0) → 1-nitro-2,4,6-tricyclohexylbenzene (40049-67-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: nitric acid; acetic anhydride; acetic acid / 6 h / 0 - 5 °C

With aluminum (III) chloride; nitric acid; acetic anhydride; acetic acid; In dichloromethane; 1: |Friedel-Crafts Alkylation;

DOI:10.1002/ejic.201402830

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 1-nitro-2,4,6-tricyclohexylbenzene (40049-67-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: nitric acid; acetic anhydride; acetic acid / 6 h / 0 - 5 °C

With aluminum (III) chloride; nitric acid; acetic anhydride; acetic acid; In dichloromethane; 1: |Friedel-Crafts Alkylation;

DOI:10.1002/ejic.201402830

upstream raw materials:

1-bromocyclohexane

benzene

1,3,5-tricyclohexylbenzene

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