MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2⁽¹⁺⁾*BF₄^(1-)=[MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2]BF₄

Base Information

• Chemical Name: MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2⁽¹⁺⁾*BF₄^(1-)=[MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2]BF₄
• CAS No.: 95345-46-3
• Molecular Formula: BF₄*C₅₇H₅₈BrMoN₂P₄
• Molecular Weight: 1157.64

Synonyms:

Chemical Property of MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2⁽¹⁺⁾*BF₄^(1-)=[MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2]BF₄

Chemical Property:

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Useful:

Technology Process of MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2⁽¹⁺⁾*BF₄^(1-)=[MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2]BF₄

There total 2 articles about MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2⁽¹⁺⁾*BF₄^(1-)=[MoBr(NNCH(CH₃)(CH₂)3)(((C₆H₅)2PCH₂)2)2]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.3%

sodium tetrafluoroborate (13755-29-8) + trans-bisdinitrogenbis(1,2-diphenylphosphinoethane)molybdenum(0) + 1,4-dibromopentane (626-87-9) → MoBr(NNCH(CH3)(CH2)3)(((C6H5)2PCH2)2)2(1+)*BF4(1-)=[MoBr(NNCH(CH3)(CH2)3)(((C6H5)2PCH2)2)2]BF4 (95345-46-3)

Guidance literature:

In ethanol; dichloromethane; benzene; other Radiation; dihaloalkane added to the Mo complex in benzene; stirring in vacuo under fluorescent lights for 24 h; green ppt. filtered off, washed with pentane, dissolved in a minimum CH2Cl2; addn. of NaBF4 in 5% aq. EtOH; identified by elem. anal., UV and NMR spectra;

Reference yield:

sodium tetrafluoroborate (13755-29-8) + MoBr(NN(CH2)3CH3)((C6H5)2PCH2CH2P(C6H5)2)2 (68022-28-6,73208-69-2) + 1,4-dibromopentane (626-87-9) → MoBr(NNCH(CH3)(CH2)3)(((C6H5)2PCH2)2)2(1+)*BF4(1-)=[MoBr(NNCH(CH3)(CH2)3)(((C6H5)2PCH2)2)2]BF4 (95345-46-3)

Guidance literature:

In not given; elem. anal.;

DOI:10.1016/S0020-1693(00)95447-1

upstream raw materials:

sodium tetrafluoroborate

MoBr(NN(CH₂)3CH₃)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

1,4-dibromopentane

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