Technology Process of 7-methyl-3-phenylbenzo[4,5]thiazolo[2,3-c][1,2,4]triazole
There total 4 articles about 7-methyl-3-phenylbenzo[4,5]thiazolo[2,3-c][1,2,4]triazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / 1,4-dioxane; mineral oil / 29 h / 20 °C / Reflux
2: sodium carbonate / water / 2 h / 90 °C / Green chemistry
3: sodium carbonate; copper(II) choride dihydrate; 1,10-Phenanthroline / water / 2 h / Green chemistry
With
1,10-Phenanthroline; copper(II) choride dihydrate; sodium hydride; sodium carbonate;
In
1,4-dioxane; water; mineral oil;
DOI:10.1039/c4gc02156h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / water / 2 h / 90 °C / Green chemistry
2: sodium carbonate; copper(II) choride dihydrate; 1,10-Phenanthroline / water / 2 h / Green chemistry
With
1,10-Phenanthroline; copper(II) choride dihydrate; sodium carbonate;
In
water;
DOI:10.1039/c4gc02156h
- Guidance literature:
-
With
1,10-Phenanthroline; copper(II) choride dihydrate; sodium carbonate;
In
water;
for 2h;
Green chemistry;
DOI:10.1039/c4gc02156h