ClGe(NC(C₆H₅)2)Cr(CO)5

Base Information

Chemical Name:ClGe(NC(C₆H₅)2)Cr(CO)5
CAS No.:115775-75-2
Molecular Formula:C₁₈H₁₀ClCrGeNO₅
Molecular Weight:480.32
Hs Code.:

ClGe(NC(C<sub>6</sub>H<sub>5</sub>)2)Cr(CO)5

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Chemical Property of ClGe(NC(C₆H₅)2)Cr(CO)5

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Technology Process of ClGe(NC(C₆H₅)2)Cr(CO)5

There total 3 articles about ClGe(NC(C₆H₅)2)Cr(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4149-28-4
bis(triethylgermyl)mercury

: Cl₂GeCr(CO)5*(C₆H₅)2CNH

: 115775-75-2
ClGe(NC(C₆H₅)2)Cr(CO)5

: mercury

Guidance literature:: In benzene; byproducts: Et3GeH, Et3GeCl; addn. of (Et3Ge)2Hg to soln. of complex in benzene, 5d, 20°C, stirred, darkness, sepn. of Hg, evapn. in reduced pressure, pptn. of powder by addn. of pentane or hexane, partial decompn., under argon; identified by IR and (1)H-NMR;
DOI:10.1016/S0022-328X(00)98909-5

Reference yield: 57.0%

: 115872-63-4
(C₂H₅)3GeNC(C₆H₅)2

: Cl₂GeCr(CO)5*C₄H₈O

: 115775-76-3
Ge(NC(C₆H₅)2)2Cr(CO)5

: 115775-75-2
ClGe(NC(C₆H₅)2)Cr(CO)5

Guidance literature:: In hexane; byproducts: Et3GeCl, THF; addn. of Et3GeNCPh2 to suspn. of Cr complex in hexane, 3h, ambient temp., equimolar ratio of educts, stirred, sepn. of ppt., washed with hexane, dried, under argon; elem. anal.;
DOI:10.1016/S0022-328X(00)98909-5

Reference yield:

: Cl₂GeCr(CO)5*(C₆H₅)2CNH

: 115775-75-2
ClGe(NC(C₆H₅)2)Cr(CO)5

: 115804-89-2
(C₂H₅)3NH⁽¹⁺⁾*Cl₂Ge(NC(C₆H₅)2)Cr(CO)5^(1-)

Guidance literature:: With triethylamine; In benzene; addn. of triethylamine to soln. of complex, 4h, 20°C, stirred, evapn. in reduced pressure, treatment of residue with THF/ether, under argon;
DOI:10.1016/S0022-328X(00)98909-5