dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)

Base Information

Chemical Name:dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)
CAS No.:69058-44-2
Molecular Formula:C₄₀H₃₈Cl₂O₄P₂Pd
Molecular Weight:822.013
Hs Code.:

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Chemical Property of dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)

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Technology Process of dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)

There total 1 articles about dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 85417-80-7
(3,4-Dimethoxyphenyl)-diphenyl-phosphin

: 69058-44-2
dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)

Guidance literature:: In dichloromethane; (N2), Pd complex in CH2Cl2 added to ligand in CH2Cl2 at room temp., stirred for 30 min; concd., treated dropwise (CH3OH), cooled in ice, collected, washed (CH3OH), dried (vac.), crystd.(diethyl ether-acetone), elem. anal.;
DOI:10.1002/ejic.200400584

Reference yield: 70.0%

: 69058-44-2
dichloropalladium(II) bis(4-(diphenylphosphanyl)veratrole)

: 10294-33-4
boron tribromide

: 861908-25-0
dipalladium(II) tetrabromo bis(4-(diphenylphosphanyl)catechol)

Guidance literature:: With water; potassium bromide; In dichloromethane; (N2), Pd complex in CH2Cl2 cooled to -80°C, treated dropwise withBBr3, warmed to room temp. overnight; quenched (H2O), diethyl ether added, org. phase washed (brine), dried, filtered, evapd., dissolved (acetone), treated with KBr, stirred for 16 h, treated with diethyl ether, org. phase washed twice, dried (MgSO4), elem. anal.;
DOI:10.1002/ejic.200400584