Fe(C₅H₄C₂C₂C₆H₅)2

Base Information

• Chemical Name: Fe(C₅H₄C₂C₂C₆H₅)2
• CAS No.: 1236297-70-3
• Molecular Formula: C₃₀H₁₈Fe
• Molecular Weight: 434.32
• Mol file: 1236297-70-3.mol

Synonyms:

Chemical Property of Fe(C₅H₄C₂C₂C₆H₅)2

Chemical Property:

Purity/Quality:

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Technology Process of Fe(C₅H₄C₂C₂C₆H₅)2

There total 1 articles about Fe(C₅H₄C₂C₂C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1,1’-bis(trimethylsilylethynyl)ferrocene + phenylacetylene (536-74-3) → C2C5H4FeC5H4C2 + Fe(C5H4C2C2C6H5)(C5H4C2Si(CH3)3) (1236297-72-5) + Fe(C5H4C2C2C6H5)2 (1236297-70-3)

Guidance literature:

With K₂CO₃; Cu(CH₃CO₂)2; In pyridine; methanol; chloroform; byproducts: 1,4-diphenyl-1,3-butadiyne; a soln. of Fe-complex, Cu(OCH3)2 and K2CO3 in CHCl3-CH3OH-pyridine 1:1:1was stirred for 15 min at 50°C, phenylacetylene in the same mixt . was added within 30 min and vigorous stirred for 10 h; concd., poured into water, filtered, extd. with CHCl3, shaken with 1 M HCl, washed with brine, dried, the solvent was removed, chromy. with hexane-CHCl3 (2:1); elem. anal.;

DOI:10.1246/bcsj.20100252

upstream raw materials:

phenylacetylene